Microstructure Investigation of Mechanically Alloyed SS316L-6Al Oxide Dispersion Strengthened Steel Powder
Abu Khalid Rivai (a*), Kandias Ahmad Muzaqi Nafsah Pratama (b), Bambang Sugeng (a)

BATAN - Badan Tenaga Nuklir Nasional
a) Center For Science and Technology of Advanced Materials - PSTBM, Kawasan Puspiptek Gd. 43, Tangerang Selatan, Banten, 15314
*rivai.abukhalid[at]batan.go.id
UNTIRTA - Universitas Sultan Ageng Tirtayasa
b) Teknik Metalurgi, Jl. Jenderal Sudirman Km 3, Kotabumi, Kec. Purwakarta, Kota Cilegon, Banten 42435

Abstract

Development of accident-tolerant fuel (ATF) cladding materials for LWR (Light Water Reactors) is being intensively carried out in many research centers in the world as the lesson-learned from the Fukushima Daiichi nuclear reactor power plant accident. One of the advanced high temperature materials which is intensively developed is Oxide Dispersion strengthened (ODS) steel. The strengthened mechanism is generate by homogeneous dispersion of nano-meter sized ceramic oxide particles in the matrix of the steel which is done by mechanical alloying technique so called mechanosynthesis. Synthesis of an austenitic ODS steel powder of SS316L with additional element of 4% aluminum and dispersion of nano-particles of 0.5% yttrium oxide (yttria: Y2O3) has been done. The aim of the research is to achieve a better performance at elevated temperature of SS316L steel as an established material for power plants. Mechanosynthesis was done using High Energy ball Milling (HEM) for 30 hours with BPR (Ball to Powder Ratio) of 10:1. Afterward, the sample was characterized using Scanning Electron Microscope-Energy Dispersive Spectroscope (SEM-EDS) and X-ray diffraction (XRD) to analyze the microstructure characteristics. The results showed that the alloying between SS316L and aluminum powders was formed. Furthermore, crystal grains and the particles of SS316L-4Al-0.5Y2O3 powder was smaller than as received SS316L and aluminum powders.

Keywords: High Temperature Materials, Steel, Microstructure, Mechanical Alloying, Oxide Dispersion Strengthened

Topic: Nuclear Science and Engineering